Plasma synthesis of Fe-based nanoparticles in low-pressure discharge
Authors | |
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Year of publication | 2010 |
Type | Article in Proceedings |
Conference | Potencial and application of nanotreatment of medical surfaces : Book of Extended Abstracts |
MU Faculty or unit | |
Citation | |
Field | Plasma physics |
Keywords | iron nanoparticles; iron pentacarbonyl; plasma; low-pressure discharge; microwave discharge |
Description | Iron-based nanoparticles in powder form were synthesised by plasmochemical method. Surface-wave discharge was sustained in low-pressure argon atmosphere by 2.45 GHz microwaves. Properties of the discharge were analysed by optical emission spectroscopy and digital photography. The nanopowder captured on filters was investigated by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The powder consisted of nanoparticles containing mainly ferrite alpha-Fe and magnetite Fe3O4. Size of synthesised nanoparticles was between 9 and 14 nm. |
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